342:
33:
730:
756:
743:
553:
In the field of surface chemistry, Emsley and co-workers introduced a new approach in the characterization of surfaces through ssNMR, called
Surface Enhanced NMR Spectroscopy (SENS). Some systems on various support materials of great chemical interest are below the sensitivity limit of detection for
507:
His team also introduced a theoretical framework for the application of continuously phase modulated radio-frequency pulses for homonuclear decoupling in solid-state NMR, allowing new families of decoupling sequences. This allowed them to obtain high-resolution proton spectra in solids. a key step
1889:
Marchetti, Alessandro; Jehle, Stefan; Felletti, Michele; Knight, Michael J.; Wang, Yao; Xu, Zhi-Qiang; Park, Ah Young; Otting, Gottfried; Lesage, Anne; Emsley, Lyndon; Dixon, Nicholas E.; Pintacuda, Guido (July 2012). "Backbone
Assignment of Fully Protonated Solid Proteins by 1H Detection and
451:
experiments, both used to improve resolution of two-dimensional heteronuclear correlation spectra through bond homonuclear correlations with the refocused INADEQUATE experiment in solids. They showed also the feasibility of ssNMR spectral editing techniques making use of heteronuclear scalar
395:
Emsley's main research field is solid-state NMR spectroscopy, specifically the development of new spectroscopic methods for the determination the atomic-level structure, the dynamics and the reactivity of a wide range of materials and molecular systems, that have been inaccessible with other
704:
355:
582:
Another subject concerns the study of paramagnetic systems, such as 4Fe-4S, high spin Fe(II) catalyst, lanthanide-containing complexes or paramagnetic centers in proteins, with specific attention to the development of NMR methods specifically aimed at paramagnetic solids.
606:
his team published some of the first ssNMR methods for the characterization of atom-specific dynamics in biosolids and its relation with solvent behaviour and function, providing detailed insight about the hierarchy of motions in proteins with the increase of temperature.
717:
558:
can be boosted using DNP, coupled with isotopic labeling and high magnetic fields. This approach enhances surface NMR signals allowing the analysis of near-surface species or materials with surface areas three orders of magnitude lower than before (around 1
334:) at the Ecole normale supérieure in Lyon, and became Full Professor in 1995. In Lyon he was the head of the Experimental Chemistry Laboratory from 1999 to 2002, and director of the Chemistry Department from 2006 to 2014. In 2002 he became a member of the
1853:
Pintacuda, Guido; Giraud, Nicolas; Pierattelli, Roberta; Böckmann, Anja; Bertini, Ivano; Emsley, Lyndon (December 2006). "Solid State NMR of a
Paramagnetic Protein: Assignment and Study of Human Dimeric Oxidized Cu(II),Zn(II) Superoxide Dismutase (SOD)".
1632:
Blanc, Frédéric; Christophe, Copéret; Lesage, Anne; Emsley, Lyndon (2008). "High resolution solid state NMR spectroscopy in surface organometallic chemistry: access to molecular understanding of active sites of well-defined heterogeneous catalysts".
1143:
Blanc, Frédéric; Copéret, Christophe; Lesage, Anne; Lyndon, Emsley (2008). "High resolution solid state NMR spectroscopy in surface organometallic chemistry: access to molecular understanding of active sites of well-defined heterogeneous catalysts".
570:
Through DNP, transfer of polarization and relevant signal enhancement can occur from the protons of the solvent batch to the rarer nuclei at natural isotopic abundance on the surface framework, including species covalently bonded to the latter one.
540:
Emsley and co-workers have shown that multi-dimensional solid state NMR can be exploited to chemically and structurally characterize catalytic surface species at a molecular level, such as reaction intermediates and catalytic centres of
1696:
Lesage, Anne; Lelli, Moreno; Gajan, David; Caporini, Marc A.; Vitzthum, Veronika; Miéville, Pascal; Alauzun, Johan; Roussey, Arthur; Thieuleux, Chloé; Geoffrey, Ahmad; Bodenhausen, Geoffrey; Coperet, Christophe; Emsley, Lyndon (2010).
1413:
Brown, S. P.; Torralba, M. P.; Sanz, D.; Claramunt, R. M.; Emsley, Lyndon (January 2002). "The Direct
Detection of a Hydrogen Bond in the Solid State by NMR through the Observation of a Hydrogen-Bond Mediated 15Nâ15N J Coupling".
251:
1545:
Sakellariou, Dimitris; Brown, Steven P.; Lesage, Anne; Hediger, Sabine; Bardet, Michel; Meriles, Carlos A.; Pines, Alexander; Emsley, Lyndon (2003). "High
Resolution NMR Correlation Spectra of Disordered Solids".
422:
barrier. CRMN was also one of the first laboratories in the world to install a high field (800 MHz proton resonant frequency) solid state DNP accessory and to test the new very fast 0.7 mm MAS rotors.
1170:
Lyndon and Anne have been developing new NMR methods for the study of the structure and dynamics of a wide range of solidstate compounds at the
Chemistry Department of the Ecole Normale Supérieure de Lyon (ENS
728:, Lyndon Emsley; Dimitri Sakellariou & Anne Lesage et al., "Method to improve resolution of two-dimensional heteronuclear correlation spectra in solid-state NMR", issued 6 February 2001
320:
741:, Sabine Hediger; Lyndon Emsley & Jay Baltisberger, "METHOD AND INSTALLATION FOR MULTI-DIMENSIONAL INHOMOGENEOUS-FIELD MAGNETIC RESONANCE IMAGING", issued 14 October 2004
387:
In 2015 he received the Bourke award "for the development of experimental methods that have transformed the field of solid-state NMR and enabled new applications across chemistry".
1777:
Crozet, M.; Chaussade, M.; Bardet, M.; Emsley, L.; Lamotte, B.; Mouesca, J. M. (2000). "13 C Solid State NMR Studies on
Synthetic Model Compounds of Clusters in the 2+ State".
1736:
Sangodkar, Rahul P.; Smith, Benjamin J.; Gajan, David; Rossini, Aaron J.; Roberts, Lawrence R.; Funkhouser, Gary P.; Lesage, Anne; Emsley, Lyndon; Chmelka, Bradley F. (2015).
1449:
Sakellariou, Dimitris; Lesage, Anne; Hodgkinson, Paul; Emsley, Lyndon (March 2000). "Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation".
2319:
501:
1340:
596:
436:
1291:
628:
the possibility to use ssNMR on a whole organism for the understanding of its metabolic pattern and the influence of drug assumption or genetic modifications.
525:
Contrary to X-ray, single crystals are not necessary with ssNMR and structural information can be obtained from high-resolution spectra of disordered solids.
455:
These implementations paved the way to the spectral characterization of solid samples at natural isotopic abundance, in a manner similar to liquid-state NMR.
683:
227:
121:
616:
754:, "POROUS AND STRUCTURED MATERIALS FOR DYNAMIC NUCLEAR POLARIZATION, PROCESS FOR THEIR PREPARATION AND NMR ANALYSIS METHOD", issued 6 August 2015
603:
592:
444:
2367:
2296:
2289:
419:
291:
working with NMR spectroscopy of solutions. Before beginning his Ph.D., he had worked more than one year in Great
Britain at a firm specializing in
2011:
Blaise, Benjamin J.; Giacomotto, Jean; Elena, Bénédicte; Marc-Emmanuel, Dumas; Toulhoat, Pierre; Ségalat, Laurent; Emsley, Lyndon (December 2007).
1263:
2273:
1121:
215:
162:
1484:
Lesage, Anne; Luminita, Duma; Sakellariou, Dimitris; Emsley, Lyndon (2001). "Improved
Resolution in Proton NMR Spectroscopy of Powdered Solids".
1386:
Lesage, Anne; Steuernagel, Stefan; Emsley, Lyndon (1998). "Carbon-13 Spectral
Editing in Solid-State NMR Using Heteronuclear Scalar Couplings".
308:
458:
It was therefore possible use scalar couplings to probe weak bonding interactions in solids and provide the first ever direct detection of a
599:, with a progressive introduction thanks to ultra-fast MAS of direct proton acquisition mimicking the sequences used for liquid NMR spectra.
522:
The improvements in the area of proton ssNMR, specifically homonuclear decoupling, set the field for the development of NMR Crystallography.
1589:
Salager, Elodie; Stein, Robin S.; Pickard, Chris J.; Elena, Bénédicte; Emsley, Lyndon (April 2009). "Powder NMR crystallography of thymol".
1520:
574:
Thanks to the description of physicochemically distinct adsorption interactions, new insights can also be offered in hydratation phenomena.
1317:
1028:
1020:
528:
In 2009 Emsley's group showed the possibility of total structure determination of drug-sized organic molecules through the combination of
2382:
414:. In 2010, under his supervision as Scientific Director, the CRMN acquired and began using the world's most powerful currently operating
702:, Lyndon Emsley & Geoffrey Bodenhausen, "Verfahren zum selektiven Anregen von nmr-Signalen", issued 31 May 1990
517:
280:
86:
2220:
989:
1361:
367:
260:
207:
108:
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211:
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1234:
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795:
2092:
2118:
821:
1067:
670:
360:
335:
219:
127:
508:
for three-dimensional structure determination of organic and inorganic materials at natural isotopic abundance.
239:
1983:
1187:
595:
in solid phase, including preparations of micro-crystalline samples, role of solvent, paramagnetic systems and
380:
In June 2014 he moved to the EPFL as a professor of Physical Chemistry, where he is currently director of the
341:
1088:
878:
1063:
715:, Lyndon Emsley & Geoffrey Bodenhausen, "Gauss-Impuls-Kaskade", issued 13 June 1991
648:
400:
359:(CRMN, European Laboratory for Very High Field NMR), which was the first step in launching the forthcoming
751:
2300:
738:
882:
404:
231:
1812:
Lesage, A.; Gardiennet, C.; Loquet, A.; Verel, R.; Emsley, L.; Meier, B.H.; Böckmann, A. (July 2008).
725:
2357:
1675:
529:
272:
284:
91:
312:
223:
542:
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1033:
624:
1116:
724:
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473:
304:
292:
148:
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2024:
1941:
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1458:
440:
288:
174:
1671:
1212:
8:
993:
463:
2028:
1945:
1790:
1738:"Influences of Dilute Organic Adsorbates on the Hydration of Low-Surface-Area Silicates"
1602:
1462:
2047:
2012:
1965:
1571:
1268:
462:
in the solid-state, as well as the first experimental demonstration of the presence of
411:
2144:
1470:
904:
Welter, Kira; Geldeard, Lynsey; Lawrence, Kate; Heydenrych, Greta (30 December 2014).
2253:
2052:
1957:
1907:
1871:
1835:
1759:
1718:
1650:
1614:
1563:
1501:
1431:
1161:
971:
927:
712:
641:
276:
1969:
399:
He published articles in NMR crystallography, structural biology, protein dynamics,
2042:
2032:
1949:
1899:
1863:
1825:
1794:
1749:
1710:
1642:
1606:
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1423:
1395:
1153:
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917:
415:
256:
169:
1313:
555:
316:
63:
637:
1991: Fellow of the Miller Institute for Basic Research in Science, Berkeley, CA
2249:
620:
2070:
1925:
Lewandowski, J.; ChHalseaussade, M.E.; Blackledge, M.; Emsley, L. (May 2015).
2346:
459:
345:
The newly completed ISA area in August 2012; the CRMN building is on the left
2165:
2037:
1953:
2096:
2056:
1961:
1911:
1903:
1875:
1867:
1839:
1830:
1813:
1763:
1722:
1654:
1618:
1567:
1505:
1435:
1165:
975:
931:
922:
905:
737:
560:
350:
245:
152:
1814:"Polarization Transfer over the Water Protein Interface in Solid Proteins"
2122:
1924:
1754:
1737:
432:
846:
470:
1798:
1714:
1559:
1497:
1427:
1399:
591:
The CRMN was one of the groups developing tools and protocols for the
435:
to introduce new through-bond carbon-proton correlation techniques in
1646:
1610:
1264:"Imagerie médicale : vers un diagnostic à moindre risque ?"
1157:
356:
Centre Européen de Résonance Magnétique Nucléaire à TrÚs Hauts Champs
315:, Berkeley), where he was introduced to solid-state NMR working with
243:
from 2008 to 2010. He is a member of the Editorial Advisory Board of
966:
949:
660:
2011: Honorary Member, National Magnetic Resonance Society of India.
327:, where he worked as a post-doc with Claude Roby and Michel Bardet.
1988:
1699:"Surface Enhanced NMR Spectroscopy by Dynamic Nuclear Polarization"
1341:"Surface Enhanced NMR Spectroscopy by Dynamic Nuclear Polarisation"
349:
In 2003 Emsley was appointed as project leader for the creation in
324:
2013:"Metabotyping of Caenorhabditis elegans reveals latent phenotypes"
2010:
1852:
1698:
1448:
711:
698:
467:
363:(ISA). The building of the new laboratory was completed in 2008.
906:"A Bright Year for Physical Chemistry â Editorial Board Renewal"
903:
657:
2011: Fellow of the International Society of Magnetic Resonance.
586:
32:
1483:
1239:
384:
of the ISIC (Institute of chemical sciences and engineering).
1544:
210:(born 29 November 1964) is a British chemist specialising in
2269:
2221:"L'académie des sciences distingue deux chercheurs lyonnais"
1888:
663:
2012: Senior Member of the Institut Universitaire de France.
189:
1984:"Waking proteins up from deep sleep to study their motions"
1811:
1776:
1631:
1213:"Waking proteins up from deep sleep to study their motions"
1032:(in French). 9 October 2010. pp. 20â21. Archived from
564:
448:
1735:
1412:
654:
2010: Luigi Sacconi Medal of the Italian Chemical Society.
1695:
1588:
1142:
651:
Award for Outstanding Achievement in Magnetic Resonance.
548:
1385:
410:
His work has involved several collaborations with the
1927:"Direct observation of hierarchical protein dynamics"
476:
330:
In October 1994 he was appointed to a Professorship (
321:
French National Laboratory for Atomic Energy Research
271:
Emsley is the son of professor James Emsley, of the
879:"Bourke Award 2015 Winner. Professor Lyndon Emsley"
796:"Lyndon Emsley nommé membre de l'Academia Europaea"
593:
structural and dynamic characterization of proteins
366:Since 2011, he has been an Associate Editor of the
1890:Ultrafast Magic-Angle-Spinning NMR Spectroscopy".
495:
1181:
1179:
1110:
1108:
2344:
373:In 2012 he was promoted to Senior Member of the
237:He was an editorial board member of the journal
1362:"éçšäșè¶
ćż«ééè§èȘæç 111 kHz æąć€Ž NMR ćæäžșçç©ćșäœćææćæ枊æ„ć
šæ°è§è§Ł"
1235:"Forscher schauten Proteinen bei der Arbeit zu"
950:"Chemistry: Breaking the billion-hertz barrier"
688:2015: Fellow of the Royal Society of Chemistry.
216:EPFL (Ăcole Polytechnique FĂ©dĂ©rale de Lausanne)
1290:RĂŒegg, Peter (30 September 2014). ethz (ed.).
1188:"Crystal clear method for identifying powders"
1176:
1105:
873:
871:
869:
867:
679:2013: Elected Member of the Academia Europaea.
676:2013: European Research Council Advanced Grant
309:Miller Institute for Basic Research in Science
1666:
1664:
1381:
1379:
587:Solid-state NMR of proteins and bioaggregates
2071:"Lyndon Emsley, médaille d'argent CNRS 2005"
1338:
1318:Centre national de la recherche scientifique
1029:Centre national de la recherche scientifique
1015:
1013:
1011:
947:
426:
403:(DNP) enhanced surface NMR spectroscopy and
1512:
1314:"Le spectromĂštre le plus puissant au monde"
1114:
992:. www.paris-en-resonance.fr. Archived from
864:
775:
773:
1661:
1376:
1292:"Bessere Auflösung dank Hyperpolarisation"
518:Nuclear magnetic resonance crystallography
281:Imperial College of Science and Technology
87:Imperial College of Science and Technology
2368:Fellows of the Royal Society of Chemistry
2185:
2046:
2036:
1829:
1753:
1008:
965:
921:
2274:Ăcole Polytechnique FĂ©dĂ©rale de Lausanne
1742:Journal of the American Chemical Society
1703:Journal of the American Chemical Society
1185:
1122:Ăcole Polytechnique FĂ©dĂ©rale de Lausanne
943:
941:
770:
368:Journal of the American Chemical Society
340:
283:in 1986 and received his Ph.D. from the
261:Journal of the American Chemical Society
163:Ăcole Polytechnique FĂ©dĂ©rale de Lausanne
1976:
1518:
577:
2345:
1058:
1056:
1054:
511:
266:
252:Solid State Nuclear Magnetic Resonance
212:solid-state nuclear magnetic resonance
114:Member of the Academia Europaea (2013)
1339:Emsley, Lyndon; Lesage, Anne (2010).
1289:
1261:
1186:Robinson, Philip (26 February 2009).
938:
631:
610:
549:DNP-enhanced surface NMR spectroscopy
788:
535:
1672:"Surface Enhanced NMR Spectroscopy"
1283:
1051:
382:Laboratoire de résonance magnétique
13:
2383:British expatriates in Switzerland
1115:Evangelista, Sandy (25 May 2015).
275:. The younger Emsley received his
14:
2399:
2326:. 28 October 2013. Archived from
2242:
1519:Bradley, David (15 August 2005).
1262:Loumé, Lise (30 September 2014).
1192:Highlights in Chemical Technology
466:in surface species, indicated by
1117:"Nominations of EPFL professors"
1068:Institut Universitaire de France
800:Ăcole normale supĂ©rieure de Lyon
671:Grand Prix Charles-Leopold Mayer
375:Institut Universitaire de France
361:Institute of Analytical Sciences
336:Institut Universitaire de France
220:Grand Prix Charles-Leopold Mayer
128:Grand Prix Charles-Leopold Mayer
31:
2213:
2179:
2158:
2137:
2111:
2085:
2063:
2004:
1918:
1882:
1846:
1805:
1770:
1729:
1689:
1625:
1582:
1538:
1477:
1442:
1406:
1354:
1332:
1306:
1255:
1227:
1205:
1136:
1081:
682:2015: Bourke Award 2015 of the
287:in 1991 under the direction of
240:Magnetic Resonance in Chemistry
982:
897:
839:
814:
784:. 27 October 2015. p. 57.
1:
2388:University of Lausanne alumni
1471:10.1016/S0009-2614(00)00127-5
948:Bhattacharya, Ananyo (2010).
764:
431:Emsley worked with colleague
2363:Members of Academia Europaea
2227:(in French). 16 October 2012
2121:(in Italian). Archived from
673:of the Académie des Sciences
554:the technique, but such low
401:dynamic nuclear polarization
7:
2378:People from Durham, England
2093:"Previous Award Recipients"
1243:(in German). 5 January 2015
390:
10:
2404:
2186:Konovalov, Alexey (2012).
883:Royal Society of Chemistry
826:Royal Society of Chemistry
692:
684:Royal Society of Chemistry
515:
319:. In 1993 he moved to the
232:Royal Society of Chemistry
218:. He was awarded the 2012
1676:European Research Council
1021:"Medailles d'argent 2005"
752:US Patent 20150219734
530:density functional theory
427:Solid-state NMR sequences
298:
273:University of Southampton
184:
180:
168:
158:
144:
137:
101:
79:
71:
42:
30:
23:
2290:"Lyndon Emsley Short CV"
2145:"The ISMAR Organization"
2119:"Medaglia Luigi Sacconi"
1521:"Crystallography by NMR"
822:"Our 2015 award winners"
739:WO Patent 2004088332
567:, instead of 1000 m/g).
313:University of California
2073:(in French). March 2006
2038:10.1073/pnas.0707393104
1954:10.1126/science.aaa6111
543:heterogeneous catalysts
496:{\displaystyle J_{C-H}}
2299:. 2010. Archived from
2297:KAUST Catalysis Center
1904:10.1002/anie.201203124
1868:10.1002/anie.200603093
1831:10.1002/anie.200801110
1591:Phys. Chem. Chem. Phys
990:"Geoffrey Bodenhausen"
923:10.1002/cphc.201402817
625:Caenorhabditis elegans
602:In collaboration with
497:
443:NMR, namely the MAS-J-
346:
285:Université de Lausanne
279:in chemistry from the
92:Université de Lausanne
2270:"Prof. Lyndon Emsley"
2017:Proc. Natl. Acad. Sci
847:"Prof. Lyndon Emsley"
726:US Patent 6184683
713:DE Patent 3940633
700:DE Patent 3839820
619:Emsley showed on the
597:sequential assignment
532:and solid-state NMR.
498:
344:
305:postdoctoral research
293:intellectual property
224:Académie des Sciences
149:Solid-state chemistry
2188:"Conference reports"
1755:10.1021/jacs.5b00622
578:Paramagnetic systems
474:
464:agostic interactions
396:analytical methods.
289:Geoffrey Bodenhausen
175:Geoffrey Bodenhausen
2029:2007PNAS..10419808B
2023:(50): 19808â19812.
1946:2015Sci...348..578L
1898:(43): 10756â10759.
1791:2000JPCA..104.9990C
1709:(44): 15459â15461.
1603:2009PCCP...11.2610S
1463:2000CPL...319..253S
1089:"ASSOCIATE EDITORS"
666:2012: AMPERE Prize.
512:NMR Crystallography
418:, which breaks the
267:Birth and education
214:and a professor at
205:David Lyndon Emsley
47:David Lyndon Emsley
2276:. 27 November 2014
2166:"Honorary Members"
1785:(44): 9990â10000.
1269:Sciences et Avenir
996:on 5 February 2016
780:"Fellows (FRSC)".
632:Honours and awards
611:Whole organism NMR
493:
412:Bruker Corporation
347:
332:Professeur associé
2256:. 28 October 2013
2254:Academia Europaea
1824:(31): 5851â5854.
1799:10.1021/jp002005o
1748:(25): 8096â8112.
1715:10.1021/ja104771z
1560:10.1021/ja0292389
1554:(14): 4376â4380.
1498:10.1021/ja0039740
1492:(24): 5747â5752.
1428:10.1021/ja0172262
1400:10.1021/ja981019t
1394:(28): 7095â7100.
960:(7281): 605â606.
802:. 23 October 2013
642:CNRS Silver Medal
604:Martin Blackledge
536:Surface catalysis
303:Emsley began his
277:Master of Science
202:
201:
139:Scientific career
2395:
2358:British chemists
2339:
2337:
2335:
2315:
2313:
2311:
2305:
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2283:
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2211:
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2141:
2135:
2134:
2132:
2130:
2115:
2109:
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2106:
2104:
2099:on 29 April 2020
2095:. Archived from
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2061:
2060:
2050:
2040:
2008:
2002:
2001:
1999:
1997:
1980:
1974:
1973:
1940:(6234): 578â81.
1931:
1922:
1916:
1915:
1886:
1880:
1879:
1862:(7): 1079â1082.
1850:
1844:
1843:
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1809:
1803:
1802:
1779:J. Phys. Chem. A
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1647:10.1039/B612793M
1629:
1623:
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1611:10.1039/b821018g
1586:
1580:
1579:
1548:J. Am. Chem. Soc
1542:
1536:
1535:
1533:
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1516:
1510:
1509:
1486:J. Am. Chem. Soc
1481:
1475:
1474:
1457:(3â4): 253â260.
1451:Chem. Phys. Lett
1446:
1440:
1439:
1422:(7): 1152â1153.
1416:J. Am. Chem. Soc
1410:
1404:
1403:
1388:J. Am. Chem. Soc
1383:
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1371:
1369:
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1347:
1336:
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1329:
1327:
1325:
1320:. 9 October 2010
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1892:Angew. Chem
1856:Angew. Chem
1818:Angew. Chem
1294:(in German)
851:www.epfl.ch
452:couplings.
433:Anne Lesage
255:. He is an
72:Nationality
2347:Categories
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2225:Le ProgrĂšs
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1128:13 January
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831:21 October
765:References
516:See also:
447:and MAS-J-
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782:The Times
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1989:Phys.org
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353:of the
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196:/emsley
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295:law.
192:.epfl
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