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Calibration

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called a limited calibration. But if the final measurement requires 10% accuracy, then the 3% gauge never can be better than 3.3:1. Then perhaps adjusting the calibration tolerance for the gauge would be a better solution. If the calibration is performed at 100 units, the 1% standard would actually be anywhere between 99 and 101 units. The acceptable values of calibrations where the test equipment is at the 4:1 ratio would be 96 to 104 units, inclusive. Changing the acceptable range to 97 to 103 units would remove the potential contribution of all of the standards and preserve a 3.3:1 ratio. Continuing, a further change to the acceptable range to 98 to 102 restores more than a 4:1 final ratio.
799: 790: 109:(BIPM) is the following: "Operation that, under specified conditions, in a first step, establishes a relation between the quantity values with measurement uncertainties provided by measurement standards and corresponding indications with associated measurement uncertainties (of the calibrated instrument or secondary standard) and, in a second step, uses this information to establish a relation for obtaining a measurement result from an indication." 674: 431:
uncertainty of all of the standards involved is considered to be insignificant when the final measurement is also made with the 4:1 ratio. This ratio was probably first formalized in Handbook 52 that accompanied MIL-STD-45662A, an early US Department of Defense metrology program specification. It was 10:1 from its inception in the 1950s until the 1970s, when advancing technology made 10:1 impossible for most electronic measurements.
699:, i.e. they had the same units as the quantity being measured. Examples include length using a yardstick and mass using a weighing scale. At the beginning of the twelfth century, during the reign of Henry I (1100-1135), it was decreed that a yard be "the distance from the tip of the King's nose to the end of his outstretched thumb." However, it wasn't until the reign of Richard I (1197) that we find documented evidence. 579: 367:" when used within the stated environmental conditions over some reasonable period of time. Having a design with these characteristics increases the likelihood of the actual measuring instruments performing as expected. Basically, the purpose of calibration is for maintaining the quality of measurement as well as to ensure the proper working of particular instrument. 733: 518:. These procedures capture all of the steps needed to perform a successful calibration. The manufacturer may provide one or the organization may prepare one that also captures all of the organization's other requirements. There are clearinghouses for calibration procedures such as the Government-Industry Data Exchange Program (GIDEP) in the United States. 587:
the instrument. There also are labels showing the date of the last calibration and when the calibration interval dictates when the next one is needed. Some organizations also assign unique identification to each instrument to standardize the record keeping and keep track of accessories that are integral to a specific calibration condition.
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would be the calibration standard. For measurement of indirect quantities of pressure per unit area, the calibration uncertainty would be dependent on the density of the manometer fluid, and the means of measuring the height difference. From this other units such as pounds per square inch could be inferred and marked on the scale.
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organization generally assigns the actual calibration interval, which is dependent on this specific measuring equipment's likely usage level. The assignment of calibration intervals can be a formal process based on the results of previous calibrations. The standards themselves are not clear on recommended CI values:
419:"... shall be calibrated at periodic intervals established and maintained to assure acceptable accuracy and reliability...Intervals shall be shortened or may be lengthened, by the contractor, when the results of previous calibrations indicate that such action is appropriate to maintain acceptable reliability." 547:
More commonly, a calibration technician is entrusted with the entire process and signs the calibration certificate, which documents the completion of a successful calibration. The basic process outlined above is a difficult and expensive challenge. The cost for ordinary equipment support is generally
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Also in the example above, ideally the calibration value of 100 units would be the best point in the gauge's range to perform a single-point calibration. It may be the manufacturer's recommendation or it may be the way similar devices are already being calibrated. Multiple point calibrations are also
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The increasing need for known accuracy and uncertainty and the need to have consistent and comparable standards internationally has led to the establishment of national laboratories. In many countries a National Metrology Institute (NMI) will exist which will maintain primary standards of measurement
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As an example, a manual process may be used for calibration of a pressure gauge. The procedure requires multiple steps, to connect the gauge under test to a reference master gauge and an adjustable pressure source, to apply fluid pressure to both reference and test gauges at definite points over the
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To prevent unauthorized access to an instrument tamper-proof seals are usually applied after calibration. The picture of the oscilloscope rack shows these, and prove that the instrument has not been removed since it was last calibrated as they will possible unauthorized to the adjusting elements of
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at specific points on the scale. This is the perception of the instrument's end-user. However, very few instruments can be adjusted to exactly match the standards they are compared to. For the vast majority of calibrations, the calibration process is actually the comparison of an unknown to a known
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The next step is defining the calibration process. The selection of a standard or standards is the most visible part of the calibration process. Ideally, the standard has less than 1/4 of the measurement uncertainty of the device being calibrated. When this goal is met, the accumulated measurement
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For example, a gauge with 3% manufacturer-stated accuracy can be changed to 4% so that a 1% accuracy standard can be used at 4:1. If the gauge is used in an application requiring 16% accuracy, having the gauge accuracy reduced to 4% will not affect the accuracy of the final measurements. This is
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To communicate the quality of a calibration the calibration value is often accompanied by a traceable uncertainty statement to a stated confidence level. This is evaluated through careful uncertainty analysis. Some times a DFS (Departure From Spec) is required to operate machinery in a degraded
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In the front and back views of a Bourdon gauge on the right, applied pressure at the bottom fitting reduces the curl on the flattened pipe proportionally to pressure. This moves the free end of the tube which is linked to the pointer. The instrument would be calibrated against a manometer, which
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saw the adoption of "indirect" pressure measuring devices, which were more practical than the manometer. An example is in high pressure (up to 50 psi) steam engines, where mercury was used to reduce the scale length to about 60 inches, but such a manometer was expensive and prone to damage. This
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Maintaining a 4:1 accuracy ratio with modern equipment is difficult. The test equipment being calibrated can be just as accurate as the working standard. If the accuracy ratio is less than 4:1, then the calibration tolerance can be reduced to compensate. When 1:1 is reached, only an exact match
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The 'single measurement' device used in the basic calibration process description above does exist. But, depending on the organization, the majority of the devices that need calibration can have several ranges and many functionalities in a single instrument. A good example is a common modern
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The exact mechanism for assigning tolerance values varies by country and as per the industry type. The measuring of equipment is manufacturer generally assigns the measurement tolerance, suggests a calibration interval (CI) and specifies the environmental range of use and storage. The using
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and many others. Since the Mutual Recognition Agreement was signed it is now straightforward to take traceability from any participating NMI and it is no longer necessary for a company to obtain traceability for measurements from the NMI of the country in which it is situated, such as the
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There may be specific connection techniques between the standard and the device being calibrated that may influence the calibration. For example, in electronic calibrations involving analog phenomena, the impedance of the cable connections can directly influence the result.
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used. Depending on the device, a zero unit state, the absence of the phenomenon being measured, may also be a calibration point. Or zero may be resettable by the user-there are several variations possible. Again, the points to use during calibration should be recorded.
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The calibration process begins with the design of the measuring instrument that needs to be calibrated. The design has to be able to "hold a calibration" through its calibration interval. In other words, the design has to be capable of measurements that are "within
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span of the gauge, and to compare the readings of the two. The gauge under test may be adjusted to ensure its zero point and response to pressure comply as closely as possible to the intended accuracy. Each step of the process requires manual record keeping.
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After all of this, individual instruments of the specific type discussed above can finally be calibrated. The process generally begins with a basic damage check. Some organizations such as nuclear power plants collect "as-found" calibration data before any
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To improve the quality of the calibration and have the results accepted by outside organizations it is desirable for the calibration and subsequent measurements to be "traceable" to the internationally defined measurement units. Establishing
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pushes the liquid down the right side of the manometer U-tube, while a length scale next to the tube measures the difference of levels. The resulting height difference "H" is a direct measurement of the pressure or vacuum with respect to
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The NMI supports the metrological infrastructure in that country (and often others) by establishing an unbroken chain, from the top level of standards to an instrument used for measurement. Examples of National Metrology Institutes are
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were designed. All these would have linear calibrations using gravimetric principles, where the difference in levels was proportional to pressure. The normal units of measure would be the convenient inches of mercury or water.
387:"A calibration certificate (or calibration label) shall not contain any recommendation on the calibration interval except where this has been agreed with the customer. This requirement may be superseded by legal regulations.” 442:
This is a simplified example. The mathematics of the example can be challenged. It is important that whatever thinking guided this process in an actual calibration be recorded and accessible. Informality contributes to
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between the standard and the device being calibrated is a completely correct calibration. Another common method for dealing with this capability mismatch is to reduce the accuracy of the device being calibrated.
478: 280:). The standard instrument for each test device varies accordingly, e.g., a dead weight tester for pressure gauge calibration and a dry block temperature tester for temperature gauge calibration. 1090: 640:, with excavations revealing the use of angular gradations for construction. The term "calibration" was likely first associated with the precise division of linear distance and angles using a 1002: 691:
ounce calibration error at zero. This is a "zeroing error" which is inherently indicated, and can normally be adjusted by the user, but may be due to the string and rubber band in this case
221: 652:. These two forms of measurement alone and their direct derivatives supported nearly all commerce and technology development from the earliest civilizations until about AD 1800. 1259: 1064:. Aiken, SC: NCSL International Workshop and Symposium, under contract with the Office of Scientific and Technical Information, U.S. Department of Energy. pp. 1–2. 575:. There easily could be 200,000 combinations of settings to completely calibrate and limitations on how much of an all-inclusive calibration can be automated. 590:
When the instruments being calibrated are integrated with computers, the integrated computer programs and any calibration corrections are also under control.
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Measuring devices and instruments are categorized according to the physical quantities they are designed to measure. These vary internationally, e.g.,
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of known accuracy. Such a standard could be another measurement device of known accuracy, a device generating the quantity to be measured such as a
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state. Whenever this does happen, it must be in writing and authorized by a manager with the technical assistance of a calibration technician.
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An automatic pressure calibrator is a device that combines an electronic control unit, a pressure intensifier used to compress a gas such as
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the output or indication on a measurement instrument to agree with value of the applied standard, within a specified accuracy. For example, a
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and/or natural physical constants, the measurement standards with the least uncertainty in the laboratory, are reached. This establishes the
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is performed. After routine maintenance and deficiencies detected during calibration are addressed, an "as-left" calibration is performed.
409:"Where necessary to ensure valid results, measuring equipment shall...be calibrated or verified at specified intervals, or prior to use...” 106: 1234: 470:
Manual calibration - US serviceman calibrating a pressure gauge. The device under test is on his left and the test standard on his right.
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This article is about assessing the accuracy of a measurement device, like a scale or a ruler. For the statistical concept, see
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Quality Control Training Manual: Comprehensive Training Guide for API, Finished Pharmaceutical and Biotechnologies Laboratories
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Strictly speaking, the term "calibration" means just the act of comparison and does not include any subsequent adjustment.
397:"...shall be calibrated or verified at periodic intervals established and maintained to assure acceptable reliability..." 506:. An automatic system may also include data collection facilities to automate the gathering of data for record keeping. 860: 1519: 1491: 325:
whenever observations appear questionable or instrument indications do not match the output of surrogate instruments
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Franceschini, Fiorenzo; Galetto, Maurizio; Maisano, Domenico; Mastrogiacomo, Luca; Pralio, Barbara (6 June 2011).
1535: 765:. In the absence of differential pressure both levels would be equal, and this would be used as the zero point. 97:
The calibration standard is normally traceable to a national or international standard held by a metrology body.
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ISO 17025: "General requirements for the competence of testing and calibration laboratories" (2005), section 5.
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standards require that these traceable actions are to a high level and set out how they can be quantified.
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This definition states that the calibration process is purely a comparison, but introduces the concept of
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could be calibrated so the error of indication or the correction is determined, and adjusted (e.g. via
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as specified by a requirement, e.g., customer specification, instrument manufacturer recommendation.
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system which includes formal, periodic, and documented calibration of all measuring instruments.
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Ligowski, M.; Jabłoński, Ryszard; Tabe, M. (2011), Jabłoński, Ryszard; Březina, Tomaš (eds.),
708:"Throughout the realm there shall be the same yard of the same size and it should be of iron." 1317: 1029: 769: 495: 364: 717: 1545: 762: 180: 62: 807:
Indirect reading design showing a Bourdon tube from the front (left) and the rear (right).
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All of the information above is collected in a calibration procedure, which is a specific
8: 1398: 829: 541: 491: 277: 35: 1430: 1093:. The National Conference of Standards Laboratories (NCSL) International. Archived from 521:
This exact process is repeated for each of the standards used until transfer standards,
403: 1550: 1540: 873:– tuning, in music, means calibrating musical instruments into playing the right pitch. 614: 249: 1191: 1515: 1487: 1462: 1377: 1350: 1323: 1319:
The Science of Empire: Scientific Knowledge, Civilization, and Colonial Rule in India
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In the direct reading hydrostatic manometer design on the right, applied pressure P
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about 10% of the original purchase price on a yearly basis, as a commonly accepted
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Automatic calibration - A U.S. serviceman using a 3666C auto pressure calibrator
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and calibration seem to have been created between the ancient civilizations of
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for other factors that are considered during calibration process development.
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Foundation: The History of England from Its Earliest Beginnings to the Tudors
721: 629: 549: 381: 150: 1155:, Mechatronics: Recent Technological and Scientific Advances, p. 227, 1122:. Washington, DC: U.S. Department of Defense. 1 August 1998. Archived from 889: 774: 572: 526: 261: 176: 130: 1233:. U.S. Department of the Interior, Bureau of Reclamation. pp. 70–73. 939:
ISO 9001: "Quality management systems — Requirements" (2008), section 7.6.
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In general use, calibration is often regarded as including the process of
19:"Zeroing" redirects here. For the U.S. government antidumping duties, see 885: 773:
stimulated the development of indirect reading instruments, of which the
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which is directly or indirectly related to national standards (such as
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in relating the accuracies of the device under test and the standard.
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Calibration methods for modern devices can be manual or automatic.
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The outcome of the comparison can result in one of the following:
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Fridman, A. E.; Sabak, Andrew; Makinen, Paul (23 November 2011).
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Military Handbook: Evaluation of Contractor's Calibration System
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plus a number of derived units) which will be used to provide
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an adjustment made to correct the error to an acceptable level
561: 233: 74: 70: 578: 1349:. Springer Science & Business Media. pp. 117–118. 1346:
Distributed Large-Scale Dimensional Metrology: New Insights
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and other difficult to diagnose post calibration problems.
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Haider, Syed Imtiaz; Asif, Syed Erfan (16 February 2011).
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Faison, C. Douglas; Brickenkamp, Carroll S. (March 2004).
1461:. Springer Science & Business Media. pp. 10–11. 1199:. U.S. Department of Defense. 17 August 1984. p. 7. 740:
One of the earliest pressure measurement devices was the
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no significant error being noted on the device under test
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Procedure for Calibrating Kelvin Probe Force Microscope
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Calibration may be required for the following reasons:
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a significant error being noted but no adjustment made
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The Quality of Measurements: A Metrological Reference
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Procedure for calibrating pressure gauges (USBR 1040)
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Other standardization attempts followed, such as the
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Bland, Alfred Edward; Tawney, Richard Henry (1919).
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The words "calibrate" and "calibration" entered the
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constants) so that it shows the true temperature in
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when a specified usage (operating hours) has elapsed
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JCGM 200:2008 International vocabulary of metrology
425: 960: 313:after an instrument has been exposed to a shock, 295:after an instrument has been repaired or modified 283: 1527: 1510:Crouch, Stanley & Skoog, Douglas A. (2007). 1448: 1484:Guide to the Measurement of Pressure and Vacuum 1390: 582:An instrument rack with tamper-indicating seals 119: 1475: 909: 744:(1643), which read atmospheric pressure using 1021: 728:The early calibration of pressure instruments 567:devices can be even more costly to maintain. 272:), and, thermodynamic or thermal properties ( 1265:. King Nutronics Corporation. Archived from 352: 298:moving from one location to another location 179:is accomplished by a formal comparison to a 107:International Bureau of Weights and Measures 105:The formal definition of calibration by the 16:Check on the accuracy of measurement devices 1396: 1363: 736:Direct reading design of a U-tube manometer 1400:English Economic History: Select Documents 1027: 947: 945: 877:Precision measurement equipment laboratory 307:before and/or after a critical measurement 133:to customer's instruments by calibration. 1309: 935: 933: 742:Mercury barometer, credited to Torricelli 720:from France and the establishment of the 593: 187:in the USA), international standards, or 169: 1376:. St. Martin's Press. pp. 133–134. 1058:Simplified Calibration Interval Analysis 731: 672: 577: 477: 465: 301:when a specified time period has elapsed 73:tone, or a physical artifact, such as a 1417: 1369: 942: 1528: 930: 716:(1225) for liquid measures, until the 656:Calibration of weights and distances ( 1481: 1315: 644:and the measurement of gravitational 626:earliest known systems of measurement 510:Process description and documentation 1054: 357: 1512:Principles of Instrumental Analysis 494:used to detect desired levels in a 13: 1420:"Pressure and vacuum measurements" 1370:Ackroyd, Peter (16 October 2012). 861:Measurement Microphone Calibration 100: 14: 1562: 459:Manual and automatic calibrations 797: 788: 34:. For the geometry concept, see 1284: 1252: 1240:from the original on 2013-05-12 1218: 1206:from the original on 2014-12-04 1184: 1091:"ANSI/NCSL Z540.3-2006 (R2013)" 1071:from the original on 2007-04-18 695:Early measurement devices were 426:Standards required and accuracy 1514:. Pacific Grove: Brooks Cole. 1403:. Macmillan Company. pp.  1322:. SUNY Press. pp. 23–24. 1109: 1083: 1048: 995: 954: 284:Instrument calibration prompts 1: 1427:Physical Methods of Chemistry 1292:"the definition of calibrate" 902: 884:– a device used to calibrate 657: 554:scanning electron microscopes 523:certified reference materials 189:certified reference materials 857:Association of European NMIs 370: 310:after an event, for example 164:National Physical Laboratory 120:Modern calibration processes 7: 1418:Tilford, Charles R (1992). 817: 748:. Soon after, water-filled 349:and recording the results. 10: 1567: 1504: 666: 604: 597: 498:, and accessories such as 260:), mechanical quantities ( 195:Quality management systems 29: 18: 1429:: 106–173. Archived from 1161:10.1007/978-3-642-23244-2 1034:. CRC Press. p. 49. 552:. Exotic devices such as 353:Basic calibration process 320:sudden changes in weather 226:electromagnetic radiation 1482:CuscĂł, Laurence (1998). 835:Calibration (statistics) 669:Weights and Measures Act 32:Calibration (statistics) 25:Zeroing (disambiguation) 866:Measurement uncertainty 781:is a notable example. 244:), time and frequency ( 220:150-2G in the U.S. and 114:measurement uncertainty 1536:Accuracy and precision 1316:Baber, Zaheer (1996). 896:Systems of measurement 842:– used to calibrate a 737: 692: 600:History of measurement 594:Historical development 583: 483: 471: 278:temperature controller 197:call for an effective 170:Quality of calibration 57:values delivered by a 23:. For other uses, see 770:Industrial Revolution 735: 676: 617:, in descriptions of 581: 496:hydraulic accumulator 481: 469: 365:engineering tolerance 53:is the comparison of 1055:Bare, Allen (2006). 970:NIST Handbook 150-2G 763:atmospheric pressure 529:of the calibration. 63:calibration standard 830:Calibrated geometry 613:as recently as the 542:routine maintenance 492:pressure transducer 36:Calibrated geometry 922:2019-10-31 at the 738: 718:Mètre des Archives 704:Assize of Measures 693: 615:American Civil War 584: 484: 472: 250:ionizing radiation 1468:978-1-4614-1478-0 1383:978-1-250-01367-5 1356:978-0-85729-543-9 1329:978-0-7914-2919-8 1170:978-3-642-23244-2 1041:978-1-4398-4994-1 850:Deadweight tester 840:Color calibration 825:Calibration curve 558:gas chromatograph 358:Purpose and scope 238:sound level meter 59:device under test 1558: 1498: 1497: 1479: 1473: 1472: 1452: 1446: 1445: 1443: 1441: 1435: 1424: 1415: 1409: 1408: 1394: 1388: 1387: 1367: 1361: 1360: 1340: 1334: 1333: 1313: 1307: 1306: 1304: 1302: 1288: 1282: 1281: 1279: 1277: 1271: 1264: 1256: 1250: 1249: 1247: 1245: 1239: 1232: 1222: 1216: 1215: 1213: 1211: 1205: 1198: 1188: 1182: 1181: 1148: 1139: 1138: 1136: 1134: 1128: 1121: 1113: 1107: 1106: 1104: 1102: 1087: 1081: 1080: 1078: 1076: 1070: 1063: 1052: 1046: 1045: 1025: 1019: 1018: 1016: 1014: 999: 993: 992: 990: 988: 982: 976:. 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Index

Zeroing (trade)
Zeroing (disambiguation)
Calibration (statistics)
Calibrated geometry
measurement
metrology
measurement
device under test
calibration standard
voltage
sound
meter
International Bureau of Weights and Measures
measurement uncertainty
SI units
traceability
NPL
UK
NIST
United States
PTB
Germany
National Physical Laboratory
traceability
standard
NIST
certified reference materials
Quality management systems
metrology
ISO 9000

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